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Identify An Unknown Compound
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Identify mixture X / sodium salt:
Mixture X consists of a carboxylic acid and a neutral compound which was separated by using 2M NaOH and filtered off through a buchner funnel / flask. the sodium salt was removed and dried in a dessicator.
The alkaline filtrate was then acidified with HCL, cooled in an ice bath and then filtered off through the buchner flask / funnel.
the identity of mixture X isn't part of this assignment, but I want to add it to my report anyway as it should gain extra marks.
The carboxylic acid was identified as benzoic acid via the melting point.
So
Mixture X + NaOH => Neutral sodium salt + ??OH??
??OH?? + HCL => Benzoic acid + H2O
Can you help me identify the missing compounds in this purification experiment?
Mixture X consists of a carboxylic acid and a neutral compound which was separated by using 2M NaOH and filtered off through a buchner funnel / flask. the sodium salt was removed and dried in a dessicator.
The alkaline filtrate was then acidified with HCL, cooled in an ice bath and then filtered off through the buchner flask / funnel.
the identity of mixture X isn't part of this assignment, but I want to add it to my report anyway as it should gain extra marks.
The carboxylic acid was identified as benzoic acid via the melting point.
So
Mixture X + NaOH => Neutral sodium salt + ??OH??
??OH?? + HCL => Benzoic acid + H2O
Can you help me identify the missing compounds in this purification experiment?
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Mixture X was alkalinised and the product MIGHT have been Sodium Benzoate.
This is soluble and would be filtrable
benzoic acid I seem to remember forms a wispy ppt
second eqn is therefore
Na- Benz + Hcl ->H Benz ( ppt) + NaCl
Remeber the ion charges if your teacher doesnt like NaCl coz it look too much like a molecule as it isnt - it charges ( haha ) around as Na+ Cl-
Mixture X was alkalinised and the product MIGHT have been Sodium Benzoate.
This is soluble and would be filtrable
benzoic acid I seem to remember forms a wispy ppt
second eqn is therefore
Na- Benz + Hcl ->H Benz ( ppt) + NaCl
Remeber the ion charges if your teacher doesnt like NaCl coz it look too much like a molecule as it isnt - it charges ( haha ) around as Na+ Cl-
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